Organic Sample Pretreatment
HQ-911F Fully Automatic Online Combustion Cracking And Absorption System
HQ-911F automatic online combustion cracking absorption system can be adapted to all imported / domestic ion chromatograph, the sample in oxygen rich, high temperature environment, complete release of sulfur or halogen in the sample, and the absorption is automatically fixed into the ion chromatography system, complete the determination of sulfur compounds or the halogen form in the sample. The whole process is completely unattended, and the sample injection, combustion, cracking, absorption and injection are completed with one key to realize the rapid and reliable analysis of sulfur and halogen (F, Cl, Br and I).
Product Details
Fully met but not limited to the following domestic / international standard methods:
JIS K7392-2009------Determination of the total content of waste plastic and bromine
GB/T 37861-2019------Determination of halogen content in electronic and electrical products-ion chromatography
SNT 5254-2020------Determination of fluorine and chlorine in coal by high-temperature hydrolysis-ion chromatography
HJ/T83-2001---------Water quality can be adsorbed organic halogen (AOX) determination-ion chromatography
GBT 39285-2020----- Palladium compound analysis method Determination of chlorine content-ion chromatography
SNT 5307-2021--------Determination of fluorine, chlorine, and sulfur for petroleum products by direct combustion-ion chromatography
GBT 40111-2021--------Determination of fluorinated chlorine and sulfur content in petroleum products-combustion-ion chromatography
TCAS 318-2018--------Polymer halogen content detection for wire and cable-oxygen bomb combustion-ion chromatography method
UOP991-11-----------Burning furnace-ion chromatography system analysis to detect fluorine, chlorine and bromine in liquid organic matter
GBT 41067-2021-------Determination of sulfur, fluorine, chlorine, bromine content in graphene powder by combustion ion chromatography
DB13T 2499.2-2017------Method of determination of liquid mixtures — Part 2 simultaneous determination of total sulfur and total chlorine (ion chromatography)
ASTM D5987-96---------Determination of total fluoride in coal and coke carbon by hydrolysis extraction and ion selective electrode or ion chromatography
ASTM D7359------------Determination of total fluoride, chlorine and sulfur in aromatics and its mixture by high temperature oxidation combustion method and ion chromatography detection method
DB34T 3368.2-2019-------Methods for analysis of hazardous substances in printed circuit boards- -Part 2: Determination of halogens (chlorine and bromine) by ion chromatography
Set automatic injection-combustion-lysis-absorption-determination as one, release the labor force;
High purity inert gas continuously purge, obtain very low system blank, easy to face supertrace halogen and sulfur analysis;
Open and close cracking furnace body structure, observe and replace the cracking tube is convenient and quick;
Automatic absorption level and volume can reduce the internal standard demand, reduce pollution, improve data repeatability;
Perfluorinated compounds in the water quality / environment:
Organic perfluorinated compounds are popular water quality pollutants. After directional adsorption, under the action of CIC combustion cracking, all organic halogen compounds are released in the form of inorganic halogen ions, and the content of total organic halogen compounds is directly determined, which is a more economical and effective environmental monitoring and control method.
Halogen compounds in OLED:
Halogens in organic luminescent materials can seriously affect the life of the devices, so they are strictly limited. Through CIC combustion cracking, the matrix complexity of various materials can be ignored, and the halogen can be released effectively and quickly measured by ion chromatography.
Halogens and sulfur in the minerals:
In the smelting process, sulfur increases the chance of environmental pollution and increases the production cost of the enterprise; halogen intensifies the corrosion of equipment at high temperature. The content of halogen and sulfur in mineral raw materials can be quickly obtained through high-temperature combustion cracking, providing necessary data support for the subsequent process.
Environment: environmental water, sewage, waste plastics, soil and so on
Electronic components: printed circuit boards, resins, cables, insulation materials, OLED, etc
Fuel: gasoline, kerosene, crude oil, coal, etc
Plastic: polyethylene, polypropylene and other polymers
Colant: pigments, paint, etc
Pharmaceutical products: APIs, intermediates, preparations, etc
Food: edible oil, spices, condiments and so on
Automatic: Automatic to complete the injection, combustion cracking, absorption and injection of solid / liquid / gas samples, and realize the rapid and reliable analysis of sulfur and halogen (F, Cl, Br, I) in the sample.
Accuracy: high recovery rate, high repeatability, overall better than the semi-automatic combustion furnace
Compatibility: strong compatibility, can be connected to any brand of ion chromatograph
Good service: the origin is in Jinan, Shandong, the supply cycle is shorter, the country has multiple offices, after-sales service is more timely
Fully automatic injection controller according to the program, the solid and semi-solid samples to the evaporation, carbonization, ash, and finally in the oxygen-rich, high temperature environment (800-1100℃) and water vapor atmosphere combustion cracking, and halogen and sulfur completely released, and fixed in a specific absorption absorption (halogen in X-, total sulfur in SO42-). After the combustion-lysis-absorption process is completed, the absorption liquid is automatically pumped into the ion chromatography system to complete the determination of each halogen form and sulfur compound.
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Specification
model | HQ-911 automatic on-line combustion cracking and absorption system | HQ-911F fully automatic online combustion cracking and absorption system |
Component name | Solid-liquid integrated manual sampler | Solid-liquid integrated automatic sampler |
Sample type | Solid, liquid, and gas | Solid, liquid, and gas |
sampling method | Manual sample delivery | Automatic mechanical arm for automatic sample delivery |
Sample volume | Solid (<150mg), liquid (<1000 uL) | Solid (<150mg), liquid (<1000 uL) |
Sample position | / | Ceramic boat, 35; The sample bottle2 mL, 84 |
Cooling auxiliary | Pal air cooling | Pal air cooling |
Component name | High-temperature combustion-based cracking furnace | |
Furnace structure | Open and closed type | |
gas;gaseous fluid | Argon gas (> 99.999%); Oxygen (> 99.999%) | |
The cleavage tube | High purity quartz pipe | |
The cleavage temperature | <1200℃,±5℃ | |
Component name | Automatic gas absorber | |
Absorb the amount of liquid | The pump was injected with 5mL | |
Absorption tube volume | 10ml | |
Fixed capacity of absorption fluid | Level sensor, precision injection pump fixed volume | |
Absorption fluid transfer | High speed peristaltic pump | |
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